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Interlaminar Fracture Testing of Composites

The threat of delamination arising from in-service loading has been one of the factors in limiting the adoption of laminated composite materials in greater volume for primary structure. While other damage modes such as matrix cracks may occur first, delaminations result in larger stiffness drops and reduction in load-bearing capabilities. Delaminations may occur from interlaminar stresses arising from geometric or material discontinuities from design features, such as an edge, a hole, a dropped ply. However, they may also occur from matrix cracks or from interlaminar stresses caused by structural loading, such as in a curved laminate, or by foreign body impacts. The delamination, once initiated, will grow under fatigue loads. During delamination growth, the structural loads may be redistributed such that another delamination occurs in another location. The delaminations may continue to grow and accumulate until a structural failure occurs, such as buckling or fibre failure. Alternatively, the delamination may be arrested and the structure may maintain some integrity. Although delamination may not cause total collapse of the load-bearing properties of the component, it is usually a precursor to such an event. Therefore, knowledge of the composite's resistance to interlaminar fracture is useful not only for product development and material screening, but a generic measurement of the interlaminar fracture toughness of the composite is useful for establishing design allowables for damage tolerance analyses of composite structures.

The equipment and fixtures at MERL allow us to conduct the following preferred tests all under the conditions of fatigue, static, creep, hot/wet cold dry, elevated temperature.


Mode I
Mode II
Mode III
Mixed Mode I/II


DCB
4ENF, ELS, ENF
ECT, SCB (modified)
MMB, FPS/ADCB, CLS, stabilised MMB


Mode I DCB test


Mixed mode I/II MMB test

MERL has pioneered the development of interlaminar fracture characterisation that have helped establish interlaminar fracture mechanics in the mainstream of composite materials characterisation. This includes the development of:
  • Methods to characterise delamination growth between threshold and critical loading in fatigue
  • A method to normalise fatigue delamination growth data to account for fibre bridging
  • The influence of insert thickness in interlaminar fracture specimen design
  • The 4ENF test fixture for accurate mode II characterisation
  • A multi-station interlaminar fatigue testing machine to reduce the costs of data generation
  • Methods to characterise delamination in woven laminates
  • Methods to automate delamination modelling in complex structures
  • Methods to predict delamination onset and growth in structural components
  • Data on the influence of supersonic flight on delamination properties
  • The influence of overloads, spectrum truncation and sequence effects on delamination growth

Delamination, e.g. from overload or fatigue
 
 

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Materials Engineering Research Laboratory Limited is Wilbury Way,
Hitchin, Hertfordshire, UK, SG4 0TW.
Registered in England. Company registration number: 2015020.

Tel: +44(0)1462 427 850
Polymer Engineering, Testing, Inspection, Research and Development, UK